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Yancheng Sanhe Biochemical Co., Ltd.

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Sanhe Biochemical

1-Bromododecane

Product name 1-Bromododecane
English alias Dodecyl bromide; Lauryl bromide;
Structural formula
Molecular formula C12H25Br
Molecular weight 249.23100
Appearance Colorless Transparent Liquid
Melting point −11~−9 ℃(lit.)
Relative density 1.040 g/mL at 20 ℃
Boiling point 134-135 ℃6 mm Hg(lit.)
Water solubility Insoluble
Refractivity n20/D 1.458(lit.)
Content ≥99.0%
Moisture ≤0.05%
Stability Stable. Combustible. Incompatible with strong oxidizing agents, strong bases.
Flash point >230 °F
Vapor pressure 0.00817mmHg at 25℃
Storage The warehouse is ventilated and dried at low temperature, and stored separately from oxidants and food additives.
Use Surfactants. Mainly used in organic synthesis, it is used in medicine to synthesize disinfectants such as bromogeramide and domimifen.
Production method Obtained by the reaction of lauryl alcohol (n-dodecanol) with hydrobromic acid: add lauryl alcohol to an enamel glass reaction pot, stir and cool, and slowly add sulfuric acid. Stir for 1 hour, then add hydrobromic acid. The temperature gradually increased to 90-95 ℃, and the stirring reaction lasted for 8 hours. The reaction is complete, cool to 30 ℃ and let stand for 8 hours. Separate the acid layer, adjust the pH of the oil layer with dilute alkaline solution, remove the alkaline solution, and wash with 50% ethanol. Vacuum distillation is used to collect products from fractions at 140-200 ℃ (3.33kPa). The yield is over 90%.
UN No.  
Hazard class  
Packing group  
HS code 2903399090
Packing 200KGS/Closed steel drum
CAS # 143-15-7

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